TY - JOUR
T1 - Synthesis and X-ray crystal structure of 8,9-dimethoxy-4-methyl-3-phenyl-2,3,5,6-tetrahydropyrrolo[2,1-a]isoquinolinium iodide
AU - Bailey, T.S.
AU - Bremner, J.B.
AU - Pelosi, L.
AU - Skelton, Brian
AU - White, Allan
PY - 1995
Y1 - 1995
N2 - N-Methylation of 6,7-dimethoxy-1-(2'-phenylcyclopropyl)-3,4-dihydroisoquinoline (3b) with iodomethane in refluxing acetone gave the modified Cloke rearrangement product, 8,9-dimethoxy-4-methyl-3-phenyl-2,3,5,6-tetrahyropyrrolo [2,1-a]isoquinolinium iodide (5b), a new derivative of the pyrrolo[2,1-a]isoquinoline skeleton, together with the methiodide salt (4b) of (3b). The structure of (5b) was confirmed by X-ray crystallographic analysis.
AB - N-Methylation of 6,7-dimethoxy-1-(2'-phenylcyclopropyl)-3,4-dihydroisoquinoline (3b) with iodomethane in refluxing acetone gave the modified Cloke rearrangement product, 8,9-dimethoxy-4-methyl-3-phenyl-2,3,5,6-tetrahyropyrrolo [2,1-a]isoquinolinium iodide (5b), a new derivative of the pyrrolo[2,1-a]isoquinoline skeleton, together with the methiodide salt (4b) of (3b). The structure of (5b) was confirmed by X-ray crystallographic analysis.
U2 - 10.1071/CH9951437
DO - 10.1071/CH9951437
M3 - Article
VL - 48
SP - 1437
EP - 1445
JO - Australian Journal of Chemistry:an international journal for chemical science
JF - Australian Journal of Chemistry:an international journal for chemical science
SN - 0004-9425
ER -