Detecting irradiation defects in materials: A machine learning approach to analyze helium bubble images

Additive manufacturing technology has received significant attention in the field of nuclear materials due to its potential to improve the radiation resistance of materials and components. In our research, we propose to use 304 L stainless steel fabricated by Selective Laser Melting (SLM) as a replacement for traditional casting due to its superior performance and optimized manufacturing technique. During testing of its radiation resistance, we found that analyzing helium bubbles captured by transmission electron microscopy (TEM) is crucial for understanding and predicting material behavior under irradiation. However, this task typically involves manual counting, which is both time-consuming and prone to errors due to the fatigue of human annotators. To address this challenge, we present a novel machine learning model for automatic helium bubbles detection and counting through images. Our model leverages a fusion of traditional computer vision techniques with cutting-edge machine learning methods to achieve superior detection of helium bubbles in nuclear materials. This approach is based on two core designs: a novel generative model to generate training data and a gradient convergence layer to limit the range of parameters. Experiments show that our model outperforms previous state-of-the-art unsupervised detectors, and achieves highly accurate helium bubble segmentation in a few-shot scenario, with an F1 score typically exceeding 90 % and an average size error less than 0.1 nm. Our model achieves over 100 times more efficiency than manual counting, which takes approximately 20 s per image. Our work demonstrates a successful collaboration between the fields of material characterization and artificial intelligence (AI). By leveraging the respective strengths of material science and machine learning, we have achieved surprising results that could have a significant impact on the development of new materials and components for nuclear applications.