Crystal structure of 4,10-dimeth-oxy-13-methyl-6H,12H-6,12-epimino-dibenzo[b,f][1,5]dioxocine

Katerina V. Kasyanova, Vladimir N. Kokozay, Elena A. Buvaylo, Olga Yu Vassilyeva, Brian W. Skelton

Research output: Contribution to journalArticlepeer-review


The title compound, C17H17NO4, lacks crystallographic symmetry with one mol-ecule per asymmetric unit. The mol-ecule exists in a folded butterfly-like conformation; the benzene rings form a dihedral angle of 84.72 (7)°. The central eight-membered imino-bridged dioxocin ring adopts a twisted-boat conformation. In the crystal, inversion-related mol-ecules are linked by pairs of weak C - H...O hydrogen bonds, forming double-stranded chains parallel to the a axis.

Original languageEnglish
Pages (from-to)410-412
Number of pages3
JournalActa Crystallographica. Section E: Structure Reports Online
Publication statusPublished - 2017


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